Ebullioscopy
Procedure
Materials Required
- Water bath
- Test tube
- Thermometer
- Stirrer
Reagents
Solvent:
- Water
- Benzene
- Carbon disulfide
- Carbon Tetrachloride
- Chloroform
Solute:
- Sodium chloride
- Calcium chloride
- Aluminium chloride
- Urea
- Glucose
Procedure
- Take the test tube from the water bath.
- Select a solvent component from the list.
- Choose a known amount of solvent.
- Place the thermometer into the test tube.
- Place the test tube in the water bath.
- Click the power on button.
- Record the temperature of the solvent.
- Click the power off button.
- Take the test tube from the water bath.
- Choose the solute from the list.
- Choose its weight.
- Place the test tube in the water bath.
- Click power on button.
- Record the temperature of the solution.
- Use the boiling point of pure solvents to determine the elevation in boiling point.
Observations and Calculations
Solvent used = .....................................
Mass of the solvent = .................. g
Boiling point of the pure solvent = ............... °C
Solute used = ........................................
Mass of the solute = ................... g
Boiling point of the solution = ...................... °C
Therefore, Elevation in boiling point of the solution = ..................... °C
The van 't Hoff factor of the solute = .........................
The molar mass of the solute = ..............................
Results
Elevation in boiling point of the solution = ..................... °C
The van 't Hoff factor of the solute = .........................
The molar mass of the solute = ..............................
Points to Remember While Performing the Experiment in a Real Laboratory
- Always wear a lab coat and gloves when you are in the lab.
- When you enter the lab, switch on the exhaust fan and ensure all the chemicals and reagents required for the experiment are available.
- If reagents are not available, prepare them using the components for reagent preparation.
- Properly adjust the flame of the Bunsen burner. The correct flame is a small blue cone, not a large plume or an orange flame.
- Clean all working apparatus with chromic acid and distilled water. Ensure all apparatus are free from water droplets before beginning the experiment.
- Calibrate the electronic weighing balance before taking measurements.
- Clean all glassware with soap and distilled water.
- After completing the experiment, recap all reagent bottles.
- Switch off the lights, exhaust fan, and gas cylinder before leaving the lab.
- Discard used gloves in a designated waste bin.